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Beilstein J. Org. Chem. 2015, 11, 1105–1111, doi:10.3762/bjoc.11.124
Graphical Abstract
Scheme 1: BEDT-TTF and chiral derivatives.
Scheme 2: Synthesis of the chiral sulfones (S,S)-1 and (R,R)-1.
Figure 1: Molecular structure of (R,R)-1 (left) and (S,S)-1 (right) together with atom numbering scheme (H at...
Figure 2: Packing of (R,R)-1 in the bc plane (left) and detailed S···S interactions (only S3···S7 (−1+x, y, z...
Figure 3: Packing of (S,S)-1 in the ab plane (left) and detailed S···S intermolecular interactions within (hi...
Beilstein J. Org. Chem. 2015, 11, 966–971, doi:10.3762/bjoc.11.108
Scheme 1: Synthesis of ligand L1, self-assemblies M4L2 and M6L3.
Figure 1: X-ray crystal structures of: (a) ligand L1, (b) self-assembly M4L2. For clarity, H atoms and TfO− c...
Figure 2: 1H NMR, downfield region (α and β signals correspond respectively to α and β pyridyl protons): (a) ...
Figure 3: X-ray crystal structure of self-assembly M6L3. For clarity, H atoms and TfO− counteranions have bee...
Figure 4: Geometry (from XRD) around two Pd centers in M4L2 (a) and M6L3 (b). The exTTF moieties have been cu...
Figure 5: Cyclic voltammogram of L1 (c = 10−3 M, CH3CN/CH2Cl2 (v/v 50/50), 0.1 M n-Bu4NPF6, 100 mV·s−1, Pt), M...